5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine

Base Information

Chemical Name:5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine
CAS No.:1095362-28-9
Molecular Formula:C₂₃H₂₆N₂O₄
Molecular Weight:394.47
Hs Code.:

Synonyms:5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine

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Chemical Property of 5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine

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Technology Process of 5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine

There total 6 articles about 5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1095362-15-4
5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-4,5-dihydro-6H-pyrrolo[1,2-a][1,4]benzodiazepin-6-one

: 1095362-28-9
5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; toluene; for 5h; Reflux;
DOI:10.3987/COM-08-11436

Reference yield:

: 65057-97-8
tetrahydro-2,5-dimethoxy-2-furaldehyde dimethyl acetal

: 1095362-28-9
5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 3 h / Reflux

2: palladium 10% on activated carbon; hydrogen / ethanol / 760.05 Torr

3: 5,5-dimethyl-1,3-cyclohexadiene / 18 h / Reflux

4: lithium aluminium tetrahydride / diethyl ether; toluene / 5 h / Reflux

With lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; acetic acid; In 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; ethanol; toluene;
DOI:10.3987/COM-08-11436

Reference yield:

: 1095362-04-1
methyl 2-{2-[(3,4-dimethoxybenzylamino)methyl]pyrrol-1-yl}-4,5-dimethoxybenzenecarboxylate hydrogenoxalate

: 1095362-28-9
5-(3,4-dimethoxybenzyl)-8,9-dimethoxy-5,6-dihydro-4H-pyrrolo[1,2-a][1,4]benzozepine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / water

2: 5,5-dimethyl-1,3-cyclohexadiene / 18 h / Reflux

3: lithium aluminium tetrahydride / diethyl ether; toluene / 5 h / Reflux

With lithium aluminium tetrahydride; potassium carbonate; In 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; water; toluene;
DOI:10.3987/COM-08-11436