N-Methyl-3-phenyl-N-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-propionamide

Base Information

• Chemical Name: N-Methyl-3-phenyl-N-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-propionamide
• CAS No.: 200504-19-4
• Molecular Formula: C₂₆H₂₇NO
• Molecular Weight: 369.506

Synonyms:N-Methyl-3-phenyl-N-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-propionamide

Chemical Property of N-Methyl-3-phenyl-N-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-propionamide

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Technology Process of N-Methyl-3-phenyl-N-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-propionamide

There total 3 articles about N-Methyl-3-phenyl-N-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butyl-[2.2]paracyclophane-4-ylcarbamate (380626-41-5) → N-Methyl-3-phenyl-N-tricyclo[8.2.2.24,7]hexadeca-1(13),4,6,10(14),11,15-hexaen-5-yl-propionamide (200504-19-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 82 percent / NaH

2: 95 percent / TFA

3: 1.) MeMgBr

With methylmagnesium bromide; sodium hydride; trifluoroacetic acid;

Reference yield:

Methyl-tricyclo[8.2.2.24,7]hexadeca-1(13),4,6,10(14),11,15-hexaen-5-yl-carbamic acid tert-butyl ester (200504-34-3) → N-Methyl-3-phenyl-N-tricyclo[8.2.2.24,7]hexadeca-1(13),4,6,10(14),11,15-hexaen-5-yl-propionamide (200504-19-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / TFA

2: 1.) MeMgBr

With methylmagnesium bromide; trifluoroacetic acid;

Reference yield:

4-N-methylamino<2.2>paracyclophane (123439-13-4,123439-29-2,123439-42-9) + hydrocinnamic acid chloride (645-45-4) → N-Methyl-3-phenyl-N-tricyclo[8.2.2.24,7]hexadeca-1(13),4,6,10(14),11,15-hexaen-5-yl-propionamide (200504-19-4)

Guidance literature:

With methylmagnesium bromide; Yield given. Multistep reaction;

upstream raw materials:

4-N-methylamino<2.2>paracyclophane

hydrocinnamic acid chloride

N-tert-butyl-[2.2]paracyclophane-4-ylcarbamate

Methyl-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4,6,10⁽¹⁴⁾,11,15-hexaen-5-yl-carbamic acid tert-butyl ester

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