N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide

Base Information

Chemical Name:N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide
CAS No.:182056-00-4
Molecular Formula:C₃₃H₃₅NO₄
Molecular Weight:509.645
Hs Code.:

Synonyms:N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide

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Chemical Property of N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide

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Technology Process of N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide

There total 4 articles about N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.2%

: 59756-83-1
2-(3-(benzyloxy)phenyl)acetyl chloride

: 182055-88-5
(R)-(+)-[2-(3,4-dimethoxyphenyl)ethyl](1-phenylethyl)amine

: 182056-00-4
N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide

Guidance literature:: With sodium hydroxide; In diethyl ether; at 0 - 5 ℃; for 2h;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 182056-00-4
N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂

2: 97.8 percent / 5percent aq. Na₂CO₃ / diethyl ether / 1 h / 0 - 5 °C

3: BF₃*OEt₂, BH₃ / tetrahydrofuran / 2.5 h / Heating

4: 87.2 percent / 5percent aq. NaOH / diethyl ether / 2 h / 0 - 5 °C

With sodium hydroxide; thionyl chloride; boron trifluoride diethyl etherate; borane; sodium carbonate; In tetrahydrofuran; diethyl ether;

Reference yield:

: 1860-58-8
3-benzyloxyphenylacetic acid

: 182056-00-4
N-[2-(3,4-dimethoxyphenyl)ethyl]-N-[(R)-1-phenylethyl]-2-(3-benzyloxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂

2: 87.2 percent / 5percent aq. NaOH / diethyl ether / 2 h / 0 - 5 °C

With sodium hydroxide; thionyl chloride; In diethyl ether;