α,α-dideuterated hydrocinnamaldehyde

Base Information

Chemical Name:α,α-dideuterated hydrocinnamaldehyde
CAS No.:29372-33-6
Molecular Formula:C₉H₁₀O
Molecular Weight:136.162
Hs Code.:

Synonyms:α,α-dideuterated hydrocinnamaldehyde

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Chemical Property of α,α-dideuterated hydrocinnamaldehyde

Chemical Property:

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Technology Process of α,α-dideuterated hydrocinnamaldehyde

There total 5 articles about α,α-dideuterated hydrocinnamaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 104-53-0
3-phenyl-propionaldehyde

: 29372-33-6
α,α-dideuterated hydrocinnamaldehyde

Guidance literature:: With dmap; water-d2; at 100 ℃; for 1h; Sealed tube;
DOI:10.1016/j.tetlet.2021.153596

Reference yield:

: 2,2'-(3-phenylpropane-1,1-diyl-2,2-d₂)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 29372-33-6
α,α-dideuterated hydrocinnamaldehyde

Guidance literature:: With sodium perborate tetrahydrate; In tetrahydrofuran; at 0 - 20 ℃; for 6h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.9b01481

Reference yield:

: 40638-92-4
1,1-dideuterio-2-phenylethanol

: 29372-33-6
α,α-dideuterated hydrocinnamaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; N-Bromosuccinimide / dichloromethane / 0 °C / Inert atmosphere; Schlenk technique

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

2.2: 1.17 h / 0 °C

3.1: sodium perborate tetrahydrate / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With N-Bromosuccinimide; sodium perborate tetrahydrate; triphenylphosphine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.9b01481