C₃₄H₂₇N₃O₇

Base Information

• Chemical Name: C₃₄H₂₇N₃O₇
• CAS No.: 1445712-31-1
• Molecular Formula: C₃₄H₂₇N₃O₇
• Molecular Weight: 589.604
• Mol file: 1445712-31-1.mol

Synonyms:C₃₄H₂₇N₃O₇

Chemical Property of C₃₄H₂₇N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₂₇N₃O₇

There total 5 articles about C₃₄H₂₇N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C26H21N3O5 (1445712-13-9) + m-anisoyl chloride (1711-05-3) → C34H27N3O7 (1445712-31-1)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jf4011033

Reference yield:

deoxypodophyllotoxin (477-51-0,6258-33-9,17187-81-4,17301-90-5,19186-35-7,24150-39-8,31892-96-3,55568-81-5,64550-41-0,69222-20-4,75171-57-2,83023-41-0,100348-38-7) → C34H27N3O7 (1445712-31-1)

Guidance literature:

Multi-step reaction with 4 steps

1: nitric acid; propionic acid / 0.07 h / 0 °C

2: chloroform / 5 h / 20 °C

3: tin(II) chloride dihdyrate / ethyl acetate / 7 h / Inert atmosphere; Reflux

4: triethylamine / dichloromethane / 0 - 20 °C

With tin(II) chloride dihdyrate; nitric acid; propionic acid; triethylamine; In dichloromethane; chloroform; ethyl acetate;

DOI:10.1021/jf4011033

Reference yield:

podofilox (518-28-5) → C34H27N3O7 (1445712-31-1)

Guidance literature:

Multi-step reaction with 5 steps

1: hydrogen; palladium 10% on activated carbon; acetic acid / 5 h / 95 °C / 1520.1 Torr

2: nitric acid; propionic acid / 0.07 h / 0 °C

3: chloroform / 5 h / 20 °C

4: tin(II) chloride dihdyrate / ethyl acetate / 7 h / Inert atmosphere; Reflux

5: triethylamine / dichloromethane / 0 - 20 °C

With tin(II) chloride dihdyrate; palladium 10% on activated carbon; hydrogen; nitric acid; acetic acid; propionic acid; triethylamine; In dichloromethane; chloroform; ethyl acetate;

DOI:10.1021/jf4011033

upstream raw materials:

C₂₆H₂₁N₃O₅

m-anisoyl chloride

podofilox

deoxypodophyllotoxin