C₃₅H₂₆BrNO₄S

Base Information

• Chemical Name: C₃₅H₂₆BrNO₄S
• CAS No.: 1374749-78-6
• Molecular Formula: C₃₅H₂₆BrNO₄S
• Molecular Weight: 636.566
• Mol file: 1374749-78-6.mol

Synonyms:C₃₅H₂₆BrNO₄S

Chemical Property of C₃₅H₂₆BrNO₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₂₆BrNO₄S

There total 4 articles about C₃₅H₂₆BrNO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H19NO2S (1374749-77-5) + ethyl 3-bromo-5-iodobenzoate (186772-44-1) → C35H26BrNO4S (1374749-78-6)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc(II) chloride; In tetrahydrofuran; at 100 ℃;

Reference yield:

C24H18BrNO2S (1374749-76-4) → C35H26BrNO4S (1374749-78-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; zinc(II) chloride; triethylamine / tetrahydrofuran / 100 °C

1.2: 20 °C

2.1: bis-triphenylphosphine-palladium(II) chloride; zinc(II) chloride; triethylamine / tetrahydrofuran / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc(II) chloride; In tetrahydrofuran;

Reference yield:

10-(prop-2-yn-1-yl)-10H-phenothiazine (4282-78-4) → C35H26BrNO4S (1374749-78-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; zinc(II) chloride; triethylamine / tetrahydrofuran / 100 °C

2.1: bis-triphenylphosphine-palladium(II) chloride; zinc(II) chloride; triethylamine / tetrahydrofuran / 100 °C

2.2: 20 °C

3.1: bis-triphenylphosphine-palladium(II) chloride; zinc(II) chloride; triethylamine / tetrahydrofuran / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc(II) chloride; In tetrahydrofuran;

upstream raw materials:

C₂₄H₁₈BrNO₂S

C₂₆H₁₉NO₂S

ethyl 3-bromo-5-iodobenzoate

10-(prop-2-yn-1-yl)-10H-phenothiazine

Downstream raw materials:

C₂₄H₁₈BrNO₂S