tert-butyl 3-[3-(benzyloxy)phenyl]propanoate

Base Information

Chemical Name:tert-butyl 3-[3-(benzyloxy)phenyl]propanoate
CAS No.:1352791-76-4
Molecular Formula:C₂₀H₂₄O₃
Molecular Weight:312.409
Hs Code.:

Synonyms:tert-butyl 3-[3-(benzyloxy)phenyl]propanoate

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Chemical Property of tert-butyl 3-[3-(benzyloxy)phenyl]propanoate

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Technology Process of tert-butyl 3-[3-(benzyloxy)phenyl]propanoate

There total 1 articles about tert-butyl 3-[3-(benzyloxy)phenyl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 540-88-5
acetic acid tert-butyl ester

: 1700-31-8
3-benzyloxybenzyl bromide

: 1352791-76-4
tert-butyl 3-[3-(benzyloxy)phenyl]propanoate

Guidance literature:: acetic acid tert-butyl ester; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -78 - -30 ℃; Inert atmosphere;

3-benzyloxybenzyl bromide; In tetrahydrofuran; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201100868

Reference yield: 83.0%

: 1352791-76-4
tert-butyl 3-[3-(benzyloxy)phenyl]propanoate

: 57668-34-5
3-(3-(benzyloxy)phenyl)propanoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 10h;
DOI:10.1002/ejoc.201100868

Reference yield:

: 1352791-76-4
tert-butyl 3-[3-(benzyloxy)phenyl]propanoate

: 1352791-77-5
tert-butyl (3R)-4-[(S)-4-benzyl-2-oxooxazolidin-3-yl]-3-[3-(benzyloxy)benzyl]-4-oxobutanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 10 h

2.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 2 h / -30 °C

2.2: 24 h

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -65 °C

3.2: 3 h / -70 °C

3.3: 12 h

With sodium hexamethyldisilazane; pivaloyl chloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201100868