methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside

Base Information

Chemical Name:methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside
CAS No.:1021954-19-7
Molecular Formula:C₂₄H₂₈O₄
Molecular Weight:380.484
Hs Code.:

Synonyms:methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside

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Technology Process of methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside

There total 1 articles about methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₀O₅S₂

: 1021954-19-7
methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2.5h; Heating;
DOI:10.1021/jo702663w

Reference yield: 47.0%

: 1021954-19-7
methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside

: 1021954-20-0
methyl (5S)-2,3-di-O-benzyl-4-deoxy-5-(2,3-dioxobutyl)-β-L-threo-pentopyranoside

Guidance literature:: methyl (5R)-2,3-di-O-benzyl-5-(2-butynyl)-4-deoxy-β-L-threo-pentopyranoside; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at -78 - 20 ℃; for 1h; Further stages.;
DOI:10.1021/jo702663w