4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

Base Information

Chemical Name:4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene
CAS No.:1362020-02-7
Molecular Formula:C₃₀H₃₆BrNSi
Molecular Weight:518.612
Hs Code.:

Synonyms:4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

Suppliers and Price of 4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

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Technology Process of 4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

There total 5 articles about 4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1362019-95-1
4-bromo-4'-(diisopropylsilyl)-E-stilbene

: 17573-94-3,752235-18-0
4-ethynyl-N,N-dimethylaniline

: 1362020-02-7
4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

Guidance literature:: With Wilkinson's catalyst; sodium iodide; In toluene; for 16h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201102031

Reference yield:

: 1362019-94-0
4-[(diisopropyl)silyl]benzaldehyde

: 1362020-02-7
4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / toluene / 12 h / Inert atmosphere; Reflux

2: Wilkinson's catalyst; sodium iodide / toluene / 16 h / Inert atmosphere; Reflux

With Wilkinson's catalyst; potassium tert-butylate; sodium iodide; In toluene;
DOI:10.1002/chem.201102031

Reference yield:

: 475160-70-4
4-(diisopropylsilanyl)-phenyl methanol

: 1362020-02-7
4-bromo-4'-[diisopropyl(4-N,N-dimethylamino-E-styryl)silyl]-E-stilbene

Guidance literature:: Multi-step reaction with 3 steps

1: manganese(IV) oxide / dichloromethane / 5 h / 20 °C / Inert atmosphere

2: potassium tert-butylate / toluene / 12 h / Inert atmosphere; Reflux

3: Wilkinson's catalyst; sodium iodide / toluene / 16 h / Inert atmosphere; Reflux

With manganese(IV) oxide; Wilkinson's catalyst; potassium tert-butylate; sodium iodide; In dichloromethane; toluene;
DOI:10.1002/chem.201102031