tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane

Base Information

• Chemical Name: tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane
• CAS No.: 236101-23-8
• Molecular Formula: C₂₄H₃₆O₄Si
• Molecular Weight: 416.633

Synonyms:tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane

Chemical Property of tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane

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Technology Process of tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane

There total 1 articles about tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tert-butyl-[3-(3-tert-butyl-4,4-dimethyl-4,5-dihydro-furan-2-ylethynyl)-phenoxy]-dimethyl-silane → tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane (236101-23-8)

Guidance literature:

With oxygen; rose bengal (adsorbed on silica gel); In dichloromethane; at -78 ℃; for 1h; Irradiation;

DOI:10.1016/S0040-4039(99)00793-5

Reference yield: 23.0%

tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane (236101-23-8) → 3-(2,2,4,4-tetramethyl-3-oxo-pentyloxycarbonylethynyl)-phenol anion

Guidance literature:

With tetrabutyl ammonium fluoride; In dimethyl sulfoxide; at 25 ℃;

DOI:10.1016/S0040-4039(99)00793-5

Reference yield:

tert-butyl-[3-(5-tert-butyl-4,4-dimethyl-2,6,7-trioxa-bicyclo[3.2.0]hept-1-ylethynyl)-phenoxy]-dimethyl-silane (236101-23-8) → [3-(tert-butyl-dimethyl-silanyloxy)-phenyl]-propynoic acid 2,2,4,4-tetramethyl-3-oxo-pentyl ester

Guidance literature:

In ⁽²⁾H₈-toluene; at 70 - 100 ℃; Activation energy;

DOI:10.1016/S0040-4039(99)00793-5

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