Technology Process of C30H22F9NO5
There total 1 articles about C30H22F9NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
at 20 ℃;
for 16h;
DOI:10.1039/c4ob00456f
- Guidance literature:
-
With
2,6-di-tert-butyl-pyridine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate;
at 155 ℃;
for 16h;
Sealed tube;
DOI:10.1039/c4ob00456f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 2,6-di-tert-butyl-pyridine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate / 16 h / 155 °C / Sealed tube
2.1: hydrogenchloride / acetonitrile / 16 h / Reflux
3.1: O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C
3.2: 16 h / Cooling with ice
With
hydrogenchloride; 2,6-di-tert-butyl-pyridine; O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c4ob00456f