1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

Base Information

Chemical Name:1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester
CAS No.:122460-22-4
Molecular Formula:C₃₁H₄₀N₂O₁₁
Molecular Weight:616.665
Hs Code.:

Synonyms:1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

Suppliers and Price of 1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

There total 4 articles about 1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 73630-07-6
1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

: 122460-22-4
1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

Guidance literature:: With pyridine; at 0 - 70 ℃;
DOI:10.1039/c2ob26888d

Reference yield:

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 122460-22-4
1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide

1.2: Heating

1.3: 2 h / 110 °C

2.1: palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / 7500.75 Torr

3.1: potassium iodide; disodium hydrogenphosphate / acetonitrile / 72 h / 90 °C

4.1: trichlorophosphate

With disodium hydrogenphosphate; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium iodide; trichlorophosphate; In ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.202100948

Reference yield:

: 52411-34-4
1,2-Bis(2-aminophenoxy)ethane

: 122460-22-4
1,2-bis(2-aminophenoxy)ethane-N,N,N'N'-tetraacetic acid tetraethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium iodide; disodium hydrogenphosphate / acetonitrile / 72 h / 90 °C

2: trichlorophosphate

With disodium hydrogenphosphate; potassium iodide; trichlorophosphate; In acetonitrile;
DOI:10.1002/ejoc.202100948