tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

Base Information

Chemical Name:tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate
CAS No.:745015-41-2
Molecular Formula:C₄₁H₆₉N₃O₁₀
Molecular Weight:764.013
Hs Code.:

Synonyms:tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

Suppliers and Price of tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

There total 5 articles about tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 794463-74-4
(S)-N²-(2-aminoethyl)-3-phenylpropane-1,2-diamine tris(hydrochloride)

: 745015-41-2
tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 5 - 50 ℃; for 49h;
DOI:10.1002/hlca.200490098

Reference yield:

: 5241-58-7
L-Phenylalanine amide

: 745015-41-2
tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 27 percent / Et₃N / acetonitrile; methanol; tetrahydrofuran / 96 h / 20 °C

2.1: trifluoroacetic acid / 5 h / 20 °C

3.1: BH₃ / tetrahydrofuran / Heating

3.2: HCl / ethanol / 2 h / cooling

4.1: 46 percent / Huenig's base / dimethylformamide / 49 h / 5 - 50 °C

With borane; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/hlca.200490098

Reference yield:

: 1510-04-9
2-[(2-aminoacetyl)amino]-3-phenylpropanamide

: 745015-41-2
tert-butyl (S)-8-benzyl-6,9,12-tris[2-(tert-butoxy)-2-oxoethyl]-2,2-dimethyl-4-oxo-3-oxa-6,9,12-triazatetradecan-14-oate

Guidance literature:: Multi-step reaction with 2 steps

1.1: BH₃ / tetrahydrofuran / Heating

1.2: HCl / ethanol / 2 h / cooling

2.1: 46 percent / Huenig's base / dimethylformamide / 49 h / 5 - 50 °C

With borane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200490098