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Technology Process of C25H36O4

C25H36O4

Base Information
  • Chemical Name:C25H36O4
  • CAS No.:1607462-63-4
  • Molecular Formula:C25H36O4
  • Molecular Weight:400.558
  • Hs Code.:
C<sub>25</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:C25H36O4

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Chemical Property of C25H36O4
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Technology Process of C25H36O4

There total 1 articles about C25H36O4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-hydroxy-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one
154714-19-9

5-hydroxy-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one

C<sub>25</sub>H<sub>36</sub>O<sub>4</sub>
1607462-63-4

C25H36O4

Guidance literature:
Multi-step reaction with 6 steps
1.1: tetrakis(triphenylphosphine) palladium(0) / dichloromethane / 0.33 h / 20 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere
3.1: dmap; pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere
4.1: 1 h / 160 °C / Inert atmosphere; Sealed tube
5.1: methanesulfonamide; AD-mix-β / tert-butyl alcohol; water / 96 h / 0 °C / Inert atmosphere; Darkness
6.1: sodium hydrogencarbonate / methanol / 6 h / 20 °C / Inert atmosphere
6.2: 1 h / Inert atmosphere; Reflux
With pyridine; dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); methanesulfonamide; AD-mix-β; sodium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol501593m
upstream raw materials:

5-hydroxy-2,2-dimethyl-4H-benzo[d][1,3]dioxin-4-one

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