C₂₅H₂₃ClF₂N₂O₃

Base Information

Chemical Name:C₂₅H₂₃ClF₂N₂O₃
CAS No.:1616291-16-7
Molecular Formula:C₂₅H₂₃ClF₂N₂O₃
Molecular Weight:472.919
Hs Code.:

C<sub>25</sub>H<sub>23</sub>ClF<sub>2</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₅H₂₃ClF₂N₂O₃

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Chemical Property of C₂₅H₂₃ClF₂N₂O₃

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Technology Process of C₂₅H₂₃ClF₂N₂O₃

There total 10 articles about C₂₅H₂₃ClF₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1303445-99-9
2-(benzyloxy)-3-(chloromethyl)-4,6-dimethylpyridine

: 1616288-75-5
8-chloro-4,4-difluoro-7-methoxy-3,4-dihydroisoquinolin-1(2H)-one

: 1616291-16-7
C₂₅H₂₃ClF₂N₂O₃

Guidance literature:: 8-chloro-4,4-difluoro-7-methoxy-3,4-dihydroisoquinolin-1(2H)-one; With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide; for 0.0833333h; Cooling with ice;

2-(benzyloxy)-3-(chloromethyl)-4,6-dimethylpyridine; In tetrahydrofuran; N,N-dimethyl-formamide; for 0.5h; Cooling with ice;

Reference yield:

: 769-28-8,70254-47-6
2-hydroxy-4,6-dimethyl-3-carbonitrile

: 1616291-16-7
C₂₅H₂₃ClF₂N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: silver(l) oxide / toluene / 20 h / 110 °C

2.1: diisobutylaluminium hydride / toluene; dichloromethane / 3 h / 0 - 20 °C

3.1: sodium tetrahydroborate; methanol / 2 h / 0 - 20 °C

4.1: thionyl chloride / dichloromethane / 0.5 h / -40 °C / Inert atmosphere

5.1: potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 0.08 h / Cooling with ice

5.2: 0.5 h / Cooling with ice

With methanol; sodium tetrahydroborate; thionyl chloride; potassium tert-butylate; diisobutylaluminium hydride; silver(l) oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 53475-53-9
2-(benzyloxy)-4,6-dimethylpyridine-3-carbonitrile

: 1616291-16-7
C₂₅H₂₃ClF₂N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / toluene; dichloromethane / 3 h / 0 - 20 °C

2.1: sodium tetrahydroborate; methanol / 2 h / 0 - 20 °C

3.1: thionyl chloride / dichloromethane / 0.5 h / -40 °C / Inert atmosphere

4.1: potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 0.08 h / Cooling with ice

4.2: 0.5 h / Cooling with ice

With methanol; sodium tetrahydroborate; thionyl chloride; potassium tert-butylate; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;