(R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone

Base Information

Chemical Name:(R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone
CAS No.:1396124-21-2
Molecular Formula:C₂₀H₂₉NO₇
Molecular Weight:395.453
Hs Code.:

Synonyms:(R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone

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Technology Process of (R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone

There total 1 articles about (R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1188522-27-1
1-morpholino-(2-O-benzyl-3,4:5,6-di-O-isopropylidene)-D-gluconamide

: 1396124-21-2
(R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone

Guidance literature:: With zinc(II) nitrate hexahydrate; In acetonitrile; at 50 ℃; for 7h;
DOI:10.1016/j.carres.2012.06.005

Reference yield:

: 1396124-21-2
(R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone

: 1396124-22-3
C₁₉H₂₅NO₆

Guidance literature:: With sodium periodate; sodium hydrogencarbonate; In dichloromethane; water; at 0 - 20 ℃;
DOI:10.1016/j.carres.2012.06.005

Reference yield:

: 1396124-21-2
(R)-2-(benzyloxy)-2-((4S,5R)-5-((R)-1,2-dihydroxyethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-1-morpholinoethanone

: 1396124-46-1
C₃₇H₅₈O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate; sodium periodate / water; dichloromethane / 0 - 20 °C

2.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C

3.2: 0 - 20 °C

4.1: tetrahydrofuran / 3 h / 10 - 15 °C / Inert atmosphere

5.1: sodium tetrahydroborate / methanol / 0.5 h / 0 - 20 °C

With sodium tetrahydroborate; sodium periodate; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.06.005