C₆₀H₇₂N₂O₁₃

Base Information

Chemical Name:C₆₀H₇₂N₂O₁₃
CAS No.:809285-87-8
Molecular Formula:C₆₀H₇₂N₂O₁₃
Molecular Weight:1029.24
Hs Code.:

C<sub>60</sub>H<sub>72</sub>N<sub>2</sub>O<sub>13</sub>

Synonyms:C₆₀H₇₂N₂O₁₃

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Chemical Property of C₆₀H₇₂N₂O₁₃

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Technology Process of C₆₀H₇₂N₂O₁₃

There total 26 articles about C₆₀H₇₂N₂O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 809285-77-6
C₆₁H₇₄N₂O₁₃

: 809285-87-8
C₆₀H₇₂N₂O₁₃

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 13.5h;
DOI:10.1021/ja0443068

Reference yield:

: 286372-15-4
(3R)-3-methoxypent-4-ynoic acid

: 809285-87-8
C₆₀H₇₂N₂O₁₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: 55 percent / 1-hydroxybenzotriazole; EDC; N-methylmorpholine / CH₂Cl₂ / 16 h / 20 °C

2.1: diethylaminosulfurtrifluoride / CH₂Cl₂ / 1 h / -78 °C

2.2: K₂CO₃ / CH₂Cl₂ / 0.67 h / -78 - 0 °C

2.3: 106.3 mg / BrCCl₃; DBU / CH₂Cl₂ / 20 h / 4 °C

3.1: 54 percent / AgNO₃; N-bromosuccinimide / acetone / 1 h / 20 °C

4.1: PdCl₂(PPh₃)2; n-Bu₄SnH / tetrahydrofuran / 3.5 h / -78 - 0 °C

4.2: 92 percent / I₂ / tetrahydrofuran

5.1: 94 percent / PdCl₂(PPh₃)2; CuI; Et₃N / acetonitrile / cooling

6.1: 80 percent / DMAP; dicyclohexylcarbodiimide / CH₂Cl₂ / 14 h / 20 °C

7.1: 94 percent / PdCl₂(PPh₃)2; CuI / acetonitrile / 1.25 h

8.1: 98 percent / aq. LiOH / tetrahydrofuran / 13.5 h / 20 °C

With 4-methyl-morpholine; dmap; bis-triphenylphosphine-palladium(II) chloride; lithium hydroxide; N-Bromosuccinimide; copper(l) iodide; diethylamino-sulfur trifluoride; n-Bu₄SnH; benzotriazol-1-ol; silver nitrate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; acetone; acetonitrile; 5.1: Sonogashira cross-coupling / 6.1: Sonogashira coupling;
DOI:10.1021/ja0443068

Reference yield:

: 809285-65-2
(3R)-5-(triisopropylsilyloxy)-1-(trimethylsilyl)pent-1-yn-3-ol

: 809285-87-8
C₆₀H₇₂N₂O₁₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: 95 percent / aq. NaOH; n-Bu₄NHSO₄ / toluene / 3.5 h / 0 - 20 °C

2.1: aq. HF / acetonitrile / 24 h / 20 °C

2.2: 99 percent / TEMPO; NaClO₂; NaOCl / aq. phosphate buffer; acetonitrile / 18 h / pH 6.7 / Heating

3.1: 55 percent / 1-hydroxybenzotriazole; EDC; N-methylmorpholine / CH₂Cl₂ / 16 h / 20 °C

4.1: diethylaminosulfurtrifluoride / CH₂Cl₂ / 1 h / -78 °C

4.2: K₂CO₃ / CH₂Cl₂ / 0.67 h / -78 - 0 °C

4.3: 106.3 mg / BrCCl₃; DBU / CH₂Cl₂ / 20 h / 4 °C

5.1: 54 percent / AgNO₃; N-bromosuccinimide / acetone / 1 h / 20 °C

6.1: PdCl₂(PPh₃)2; n-Bu₄SnH / tetrahydrofuran / 3.5 h / -78 - 0 °C

6.2: 92 percent / I₂ / tetrahydrofuran

7.1: 94 percent / PdCl₂(PPh₃)2; CuI; Et₃N / acetonitrile / cooling

8.1: 80 percent / DMAP; dicyclohexylcarbodiimide / CH₂Cl₂ / 14 h / 20 °C

9.1: 94 percent / PdCl₂(PPh₃)2; CuI / acetonitrile / 1.25 h

10.1: 98 percent / aq. LiOH / tetrahydrofuran / 13.5 h / 20 °C

With 4-methyl-morpholine; dmap; bis-triphenylphosphine-palladium(II) chloride; lithium hydroxide; sodium hydroxide; N-Bromosuccinimide; copper(l) iodide; diethylamino-sulfur trifluoride; n-Bu₄SnH; hydrogen fluoride; tetra(n-butyl)ammonium hydrogensulfate; benzotriazol-1-ol; silver nitrate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; acetone; toluene; acetonitrile; 7.1: Sonogashira cross-coupling / 8.1: Sonogashira coupling;
DOI:10.1021/ja0443068