5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

Base Information

Chemical Name:5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol
CAS No.:158895-34-2
Molecular Formula:C₅₁H₅₄O₁₁
Molecular Weight:842.983
Hs Code.:

Synonyms:5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

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Chemical Property of 5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

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Technology Process of 5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

There total 2 articles about 5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 111549-97-4
2,3,4-Tris-O-(phenylmethyl)-5-O-(prop-2-enyl)-D-ribitol

: 3-O-Allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl trichloroacetimidate

: 158895-34-2
5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

Guidance literature:: With 4 A molecular sieve; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; 1.) r.t., 30 min, 2.) 0 deg C;

Reference yield:

: 3-O-Allyl-2,5-di-O-benzoyl-α,β-D-ribofuranose

: 158895-34-2
5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / CH₂Cl₂ / 5 h

2: 80 percent / molecular sieves 4 Angstroem / trimethylsilyl triflate / CH₂Cl₂ / 1.) r.t., 30 min, 2.) 0 deg C

With 4 A molecular sieve; potassium carbonate; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;

Reference yield:

: 158895-34-2
5-O-Allyl-1-O-(3-O-allyl-2,5-di-O-benzoyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

: 118964-43-5
1-O-(2,5-Di-O-benzyl-β-D-ribofuranosyl)-2,3,4-tri-O-benzyl-D-ribitol

Guidance literature:: Multi-step reaction with 3 steps

1: MeONa / methanol / 12 h

2: NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) r.t., overnight

3: 60 percent / AcONa / PdCl₂ / aq. acetic acid / 24 h

With sodium methylate; sodium acetate; sodium hydride; palladium dichloride; In methanol; acetic acid; N,N-dimethyl-formamide;