N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

Base Information

Chemical Name:N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide
CAS No.:1248342-31-5
Molecular Formula:C₂₇H₂₇NO₃S
Molecular Weight:445.582
Hs Code.:

Synonyms:N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

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Technology Process of N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

There total 1 articles about N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1248342-30-4
(S,E)-N-(3-hydroxy-2-(naphthalen-2-yl)-3-phenylprop-1-enyl)-N,4-dimethylbenzenesulfonamide

: N-((2R,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

: 1248342-31-5
N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: With palladium hydroxide on carbon; hydrogen; In methanol; for 30h; under 760.051 Torr; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ja105435y

Reference yield: 89.0%

: 1248342-31-5
N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

: 492434-60-3
(2S,3R)-3-hydroxy-N-methyl-2-(naphthalen-2-yl)-3-phenylpropan-1-amine

Guidance literature:: N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide; With naphthalene; sodium; In 1,2-dimethoxyethane; Inert atmosphere;

With water; In 1,2-dimethoxyethane;
DOI:10.1021/ja105435y

Reference yield: 88.0%

: 1248342-31-5
N-((2S,3R)-3-hydroxy-2-(naphthalen-2-yl)-3-phenylpropyl)-N,4-dimethylbenzenesulfonamide

: 65-85-0,8013-63-6
benzoic acid

: 1248342-70-2
C₃₄H₃₁NO₄S

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ja105435y