6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Base Information

Chemical Name:6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone
CAS No.:122907-52-2
Molecular Formula:C₁₉H₂₆O₅
Molecular Weight:334.412
Hs Code.:

Synonyms:6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

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Chemical Property of 6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

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Technology Process of 6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

There total 6 articles about 6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3066-90-8
2,3-dimethoxy-5-methylbenzene-1,4-diol

: 122907-52-2
6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BF₃-ether; 2.) FeCl₃ / 1., r.t., 90 min, dioxane; 2.) 83 percent MeOH, dioxane

2: 1.) sodium borohydride; FeCl₃ / 1.) MeOH, 15 min; 2.) MeOH, water

With sodium tetrahydroborate; boron trifluoride diethyl etherate; iron(III) chloride;
DOI:10.1248/cpb.33.3745

Reference yield:

: 606-06-4
2-[(E)-3,7-dimethyl-2,6-octadienyl]-5,6-dimethoxy-3-methyl-1,4-benzoquinone

: 122907-52-2
6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: Zn

2: 15 percent / SeO₂ / aq. ethanol / 1 h / 75 - 80 °C

3: 1.) lithium aluminum hydride; 2.) FeCl₃ / 1.) Et₂O, 30 min; 2.) Et₂O, H₂O, 30 min

With lithium aluminium tetrahydride; selenium(IV) oxide; iron(III) chloride; zinc; In ethanol;
DOI:10.1248/cpb.33.3745

Reference yield:

: 52117-20-1
Acetic acid 4-acetoxy-2-((E)-3,7-dimethyl-octa-2,6-dienyl)-5,6-dimethoxy-3-methyl-phenyl ester

: 122907-52-2
6-(8-hydroxy-3,7-dimethyl-2,6-octadienyl)-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 15 percent / SeO₂ / aq. ethanol / 1 h / 75 - 80 °C

2: 1.) lithium aluminum hydride; 2.) FeCl₃ / 1.) Et₂O, 30 min; 2.) Et₂O, H₂O, 30 min

With lithium aluminium tetrahydride; selenium(IV) oxide; iron(III) chloride; In ethanol;
DOI:10.1248/cpb.33.3745