(1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

Base Information

Chemical Name:(1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine
CAS No.:1338797-29-7
Molecular Formula:C₁₇H₁₆BrNO₂
Molecular Weight:346.224
Hs Code.:

Synonyms:(1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

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Technology Process of (1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

There total 1 articles about (1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1338796-89-6
1-bromo-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-one

: 1338797-28-6
(4-bromo-6-hydroxy-1-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

: (4-bromo-6-hydroxy-1-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

: (1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

: 1338797-29-7
(1-bromo-6-hydroxy-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-yl)hydroxylimine

Guidance literature:: trimethylsilyl trifluoromethanesulfonate; 1-bromo-4-phenyl-5,6,8,9-tetrahydrobenzocyclohepten-7-one; With triethylamine; In toluene; at 80 ℃; for 4h; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 3h; optical yield given as %de; Further stages; Inert atmosphere;
DOI:10.1016/j.bmc.2011.06.089