(3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester

Base Information

• Chemical Name: (3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester
• CAS No.: 388071-37-2
• Molecular Formula: C₂₃H₃₂N₂O₄
• Molecular Weight: 400.518

Synonyms:(3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester

Chemical Property of (3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester

Chemical Property:

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Technology Process of (3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester

There total 7 articles about (3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(3S,2R) (3-azido-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester (658691-01-1) → (3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester (388071-37-2)

Guidance literature:

With hydrogen; palladium/active carbon; In methanol; under 2585.81 Torr;

Reference yield:

(3R,4S)-4-benzyloxycarbonylamino-3-hydroxy-2-(3-methoxy-benzylamino)-5-phenyl-pentanoic acid tert-butyl ester → (3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester (388071-37-2)

Guidance literature:

With hydrogen; 5%-palladium/activated carbon; In methanol; for 2h; under 2585.81 Torr;

Reference yield:

{1-benzyl-3-[tert-butoxycarbonyl-(3-methoxy-benzyl)-amino]-2-hydroxy-propyl}-carbamic acid benzyl ester (388071-36-1) → (3S)-(3-amino-2-hydroxy-4-phenyl-butyl)-(3-methoxy-benzyl)-carbamic acid tert-butyl ester (388071-37-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1016/j.bmcl.2006.09.092

upstream raw materials:

{1-benzyl-3-[tert-butoxycarbonyl-(3-methoxy-benzyl)-amino]-2-hydroxy-propyl}-carbamic acid benzyl ester

benzyl (1S,2R)-1-benzyl-2-hydroxy-3-[(3-methoxybenzyl)amino]propylcarbamate

3-METHOXYBENZYLAMINE

N-benzyloxycarbonyl-3(S)-amino-1,2(S)epoxy-4-phenylbutane

Downstream raw materials:

tert-butyl (2R,3S)-3-({3-cyano-5-[(dipropylamino)carbonyl]benzoyl}amino)-2-hydroxy-4-phenylbutyl-(3-methoxybenzyl)carbamate

C₄₉H₆₂N₄O₈

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