C₆₇H₇₅N₄O₁₇SCl₃

Base Information

Chemical Name:C₆₇H₇₅N₄O₁₇SCl₃
CAS No.:925451-85-0
Molecular Formula:C₆₇H₇₅Cl₃N₄O₁₇S
Molecular Weight:1346.77
Hs Code.:

C<sub>67</sub>H<sub>75</sub>N<sub>4</sub>O<sub>17</sub>SCl<sub>3</sub>

Synonyms:C₆₇H₇₅N₄O₁₇SCl₃

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Chemical Property of C₆₇H₇₅N₄O₁₇SCl₃

Chemical Property:

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Technology Process of C₆₇H₇₅N₄O₁₇SCl₃

There total 13 articles about C₆₇H₇₅N₄O₁₇SCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874758-58-4
3-acetoxymethyl-8-allyloxy-1-(3-tert-butoxycarbonyl-2,2-dimethyl-oxazolidin-4-yl)-7-methoxy-6-methyl-3,4-dihydro-1H-isoquinoline-2-carboxylic acid allyl ester

: 925451-85-0
C₆₇H₇₅N₄O₁₇SCl₃

Guidance literature:: Multi-step reaction with 12 steps

1.1: 91 percent / CeCl₃*7H₂O; oxalic acid / acetonitrile / 2 h / 20 °C

2.1: oxalyl chloride; dimethylsulfoxide; triethylamine / CH₂Cl₂ / -60 - 20 °C

3.1: 74 percent / CH₃MgCl / tetrahydrofuran; CH₂Cl₂ / 20 °C

4.1: 88 percent / DIPEA / CHCl₃ / 6 h / 20 - 60 °C

5.1: 2,6-lutidine; tert-butyldimethylsilyl triflate / CH₂Cl₂ / 3 h / 20 °C

5.2: 86 percent / KF monohydrate / methanol / 40 h / 20 °C

6.1: 94 percent / potassium carbonate / methanol / 1 h / 20 °C

7.1: 90 percent / acetic acid / CH₂Cl₂ / 2 h / 20 °C

8.1: oxalyl chloride; dimethylsulfoxide; triethylamine / CH₂Cl₂ / -60 - 20 °C

9.1: 378 mg / zinc(II) chloride / CH₂Cl₂; tetrahydrofuran / 0.67 h / 23 °C

10.1: 90 percent / acetic acid; zinc / diethyl ether / 1.5 h / 23 °C

11.1: 94 percent / potassium carbonate / acetonitrile / 4 h / 20 °C

12.1: 93 percent / DMAP; EDCl / CH₂Cl₂ / 1 h / 20 °C

With 2,6-dimethylpyridine; dmap; cerium(III) chloride; oxalyl dichloride; t-butyldimethylsiyl triflate; methylmagnesium chloride; oxalic acid; potassium carbonate; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; zinc; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; acetonitrile; 2.1: Swern oxidation / 7.1: Pictet-Spengler reaction / 8.1: Swern oxidation / 9.1: Strecker reaction;
DOI:10.1002/anie.200603179

Reference yield:

: 925451-95-2
C₃₆H₄₅N₃O₁₁

: 925451-85-0
C₆₇H₇₅N₄O₁₇SCl₃

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / potassium carbonate / acetonitrile / 4 h / 20 °C

2: 93 percent / DMAP; EDCl / CH₂Cl₂ / 1 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetonitrile;
DOI:10.1002/anie.200603179

Reference yield:

: 925451-76-9
C₄₃H₆₄N₂O₁₂Si

: 925451-85-0
C₆₇H₇₅N₄O₁₇SCl₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: 88 percent / DIPEA / CHCl₃ / 6 h / 20 - 60 °C

2.1: 2,6-lutidine; tert-butyldimethylsilyl triflate / CH₂Cl₂ / 3 h / 20 °C

2.2: 86 percent / KF monohydrate / methanol / 40 h / 20 °C

3.1: 94 percent / potassium carbonate / methanol / 1 h / 20 °C

4.1: 90 percent / acetic acid / CH₂Cl₂ / 2 h / 20 °C

5.1: oxalyl chloride; dimethylsulfoxide; triethylamine / CH₂Cl₂ / -60 - 20 °C

6.1: 378 mg / zinc(II) chloride / CH₂Cl₂; tetrahydrofuran / 0.67 h / 23 °C

7.1: 90 percent / acetic acid; zinc / diethyl ether / 1.5 h / 23 °C

8.1: 94 percent / potassium carbonate / acetonitrile / 4 h / 20 °C

9.1: 93 percent / DMAP; EDCl / CH₂Cl₂ / 1 h / 20 °C

With 2,6-dimethylpyridine; dmap; oxalyl dichloride; t-butyldimethylsiyl triflate; potassium carbonate; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; zinc; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; acetonitrile; 4.1: Pictet-Spengler reaction / 5.1: Swern oxidation / 6.1: Strecker reaction;
DOI:10.1002/anie.200603179