C₃₂H₂₄ClF₃N₆

Base Information Edit

Chemical Name:C₃₂H₂₄ClF₃N₆
CAS No.:1337567-04-0
Molecular Formula:C₃₂H₂₄ClF₃N₆
Molecular Weight:585.031
Hs Code.:
Mol file:1337567-04-0.mol

C<sub>32</sub>H<sub>24</sub>ClF<sub>3</sub>N<sub>6</sub>

Synonyms:C₃₂H₂₄ClF₃N₆

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Chemical Property of C₃₂H₂₄ClF₃N₆ Edit

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Technology Process of C₃₂H₂₄ClF₃N₆

There total 9 articles about C₃₂H₂₄ClF₃N₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1337567-03-9
C₂₅H₁₆Cl₂F₃N₅

: 100-46-9
benzylamine

: 1337567-04-0
C₃₂H₂₄ClF₃N₆

Guidance literature:: at 140 ℃; for 0.75h;

Reference yield:

: 100-46-9
benzylamine

: 1337567-04-0
C₃₂H₂₄ClF₃N₆

Guidance literature:: Multi-step reaction with 6 steps

1: 0.33 h / Cooling with ice

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.67 h / -78 - 20 °C

3: hydrazine / 1,4-dioxane / 1 h / 20 °C

4: boron trifluoride diethyl etherate / methanol / 1.5 h / 100 °C / sealed tube

5: ethylenediamine; copper(l) iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C

6: 0.75 h / 140 °C

With copper(l) iodide; boron trifluoride diethyl etherate; ethylenediamine; 3-chloro-benzenecarboperoxoic acid; hydrazine; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 27007-53-0
methyl-2-bromo-5-chlorobenzoate

: 1337567-04-0
C₃₂H₂₄ClF₃N₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 - 0 °C

1.2: 1 h / 20 °C

2.1: boron trifluoride diethyl etherate / methanol / 1.5 h / 100 °C / sealed tube

3.1: ethylenediamine; copper(l) iodide / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.1: 0.75 h / 140 °C

With copper(l) iodide; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; ethylenediamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;