tripropylgermanyl hydrate

Base Information

• Chemical Name: tripropylgermanyl hydrate
• CAS No.: 2237-94-7
• Molecular Formula: C18H42 Ge2 O
• Molecular Weight: 419.711
• Mol file: 2237-94-7.mol

Synonyms:Bis(tripropylgermanium)oxide (6CI); Digermoxane, hexapropyl- (8CI,9CI); Germane, oxybis[tripropyl-(7CI); Hexapropyldigermoxane; NSC 86327

Chemical Property of tripropylgermanyl hydrate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tripropylgermanyl hydrate

There total 4 articles about tripropylgermanyl hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(tripropylgermyl)butyric acid (81906-34-5) → nonyltripropylgermane (78819-05-3) + tetra-n-propylgermane (994-65-0) + Bis-(tripropylgermanium)-oxid (2237-94-7)

Guidance literature:

Multi-step reaction with 3 steps

1: neat (no solvent)

2: diethyl ether

3: nonane / further solvent(s)

With nonane; In diethyl ether;

Reference yield:

ethyl 4-(tripropylgermyl)butyrate (81906-33-4) → nonyltripropylgermane (78819-05-3) + tetra-n-propylgermane (994-65-0) + Bis-(tripropylgermanium)-oxid (2237-94-7)

Guidance literature:

Multi-step reaction with 4 steps

1: KOH / potassium hydroxide

2: neat (no solvent)

3: diethyl ether

4: nonane / further solvent(s)

With KOH; nonane; In potassium hydroxide; diethyl ether;

Reference yield:

4-(tripropylgermyl)butyryl chloride (81906-35-6) → 4-(tripropylgermyl)butyric acid (81906-34-5) + nonyltripropylgermane (78819-05-3) + tetra-n-propylgermane (994-65-0) + Bis-(tripropylgermanium)-oxid (2237-94-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: nonane / further solvent(s)

With nonane; In diethyl ether;

upstream raw materials:

tert-butyl 4-(tripropylgermyl)peroxybutyrate

4-(tripropylgermyl)butyric acid

4-(tripropylgermyl)butyryl chloride

ethyl 4-(tripropylgermyl)butyrate