4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide

Base Information

Chemical Name:4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide
CAS No.:75168-63-7
Molecular Formula:C₁₄H₉BrF₃NOS
Molecular Weight:376.197
Hs Code.:

Synonyms:4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide

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Technology Process of 4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide

There total 1 articles about 4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 45988-04-3,84452-45-9,84452-46-0
1-phenyl-2,2,2-trifluoroethylideneimine

: 75168-73-9
4-bromobenzenesulfonyl chloride

: 75168-63-7
4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide

Guidance literature:: With triethylamine; In diethyl ether; at 20 ℃; for 2h;

Reference yield: 94.0%

: 75168-63-7
4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide

: 75168-71-7
C₁₄H₉BrCl₂F₃NOS

Guidance literature:: With chlorine; In tetrachloromethane; at 20 ℃; for 24h;

Reference yield:

: 75168-63-7
4-Bromo-benzenesulfinic acid [2,2,2-trifluoro-1-phenyl-eth-(Z)-ylidene]-amide

: 75168-72-8
C₂₂H₂₅BrF₃N₃O₃S

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / chlorine / CCl₄ / 24 h / 20 °C

2: 60 percent / diethyl ether / 1 h / 20 °C

With chlorine; In tetrachloromethane; diethyl ether;