benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate

Base Information

Chemical Name:benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate
CAS No.:1380608-64-9
Molecular Formula:C₄₇H₄₀O₁₀S
Molecular Weight:796.895
Hs Code.:

Synonyms:benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate

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Chemical Property of benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate

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Technology Process of benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate

There total 3 articles about benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1380608-63-8
(2R,4S,5R)-benzyl 2-{5-[4-hydroxy-5-hydroxymethyltetrahydrofuran-2-yl]thiophen-2-yl}-4-oxo-4H-chromen-3-yl carbonate

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1380608-64-9
benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate

Guidance literature:: With pyridine; at 20 ℃; for 24h;
DOI:10.1021/ja3030388

Reference yield:

: 1332744-71-4
benzyl 2-bromo-4-oxo-4H-chromen-3-yl carbonate

: 1380608-64-9
benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / Reflux; Inert atmosphere

2: pyridine hydrogenfluoride / tetrahydrofuran

3: pyridine / 24 h / 20 °C

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; pyridine hydrogenfluoride; In tetrahydrofuran; toluene;
DOI:10.1021/ja3030388

Reference yield:

: 1380608-60-5
C₅₃H₇₄O₃SSi₂Sn

: 1380608-64-9
benzyl 2-(5-{5-[bis-(4-methoxyphenyl)phenylmethoxymethyl]-4-hydroxytetrahydrofuran-2-yl}-thiophen-2-yl)-4-oxo-4H-chromen-3-yl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / Reflux; Inert atmosphere

2: pyridine hydrogenfluoride / tetrahydrofuran

3: pyridine / 24 h / 20 °C

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; pyridine hydrogenfluoride; In tetrahydrofuran; toluene;
DOI:10.1021/ja3030388