(3ar,7at,3'ar',7'at')-Δ²,Δ^2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole

Base Information

• Chemical Name: (3ar,7at,3'ar',7'at')-Δ²,Δ^2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole
• CAS No.: 93999-71-4
• Molecular Formula: C₁₈H₂₈N₂O₂S₂
• Molecular Weight: 368.565

Synonyms:(3ar,7at,3'ar',7'at')-Δ²,Δ^2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole

Chemical Property of (3ar,7at,3'ar',7'at')-Δ²,Δ^2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole

Chemical Property:

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Technology Process of (3ar,7at,3'ar',7'at')-Δ²,Δ^2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole

There total 2 articles about (3ar,7at,3'ar',7'at')-Δ²,Δ^2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-trans-2-aminocyclohexanol (931-16-8,6850-38-0,6982-39-4,33092-82-9,38898-70-3,74111-21-0,108267-20-5,931-15-7) → (3ar,7at,3'ar',7'at')-Δ2,Δ2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole (93999-71-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / 2 h / Heating

2: KOH / ethanol / 16 h / 20 °C

With potassium hydroxide; sodium hydroxide; In ethanol;

Reference yield:

1,4-dibromo-butane (110-52-1) + (3ar,7at)-hexahydro-benzooxazole-2-thione (77425-28-6,89775-28-0) → (3ar,7at,3'ar',7'at')-Δ2,Δ2'-dodecahydro-2,2'-butane-1,4-diylbissulfanyl-bis-benzooxazole (93999-71-4)

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 16h;

upstream raw materials:

1,4-dibromo-butane

(3ar,7at)-hexahydro-benzooxazole-2-thione

(+/-)-trans-2-aminocyclohexanol

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