C₃₂H₄₅IN₂O₆Si

Base Information

Chemical Name:C₃₂H₄₅IN₂O₆Si
CAS No.:1016976-23-0
Molecular Formula:C₃₂H₄₅IN₂O₆Si
Molecular Weight:708.709
Hs Code.:

C<sub>32</sub>H<sub>45</sub>IN<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₃₂H₄₅IN₂O₆Si

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Chemical Property of C₃₂H₄₅IN₂O₆Si

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Technology Process of C₃₂H₄₅IN₂O₆Si

There total 17 articles about C₃₂H₄₅IN₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1016976-14-9
methyl 3-amino-5-benzyloxy-4-iodobenzoate

: 1016976-12-7
C₁₇H₃₁NO₄Si

: 1016976-23-0
C₃₂H₄₅IN₂O₆Si

Guidance literature:: methyl 3-amino-5-benzyloxy-4-iodobenzoate; C₁₇H₃₁NO₄Si; With acetic acid; In chloroform; at 20 ℃; for 12h; Molecular sieve; Inert atmosphere;

With sodium cyanoborohydride; In tetrahydrofuran; dichloromethane; for 2h; Inert atmosphere;
DOI:10.1021/ol800127a

Reference yield:

: 885703-19-5
(3S,4S)-4-N-phthalimido-1,5-hexadiene-3-ol

: 1016976-23-0
C₃₂H₄₅IN₂O₆Si

Guidance literature:: Multi-step reaction with 11 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 11 h / 20 °C / Inert atmosphere

2: osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 6 h / 5 °C / Inert atmosphere

3: nitrogen; methylamine / water / 1 h / 50 °C / 10 Torr / Inert atmosphere

4: sodium hydrogencarbonate / ethyl acetate / 1.5 h / Inert atmosphere

5: dmap; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.03 h / 0 - 20 °C / Inert atmosphere

6: dichloromethane / 1 h / -40 °C / Inert atmosphere

7: caesium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

8: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / Inert atmosphere

9: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

10: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

11: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

With 1H-imidazole; dmap; osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; nitrogen; tetrabutyl ammonium fluoride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; methylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; chloroform; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201003489

Reference yield:

: 1016976-13-8
3-benzyloxy-4-iodo-5-nitrobenzaldehyde

: 1016976-23-0
C₃₂H₄₅IN₂O₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: N-iodo-succinimide; potassium carbonate / acetonitrile / 12 h / 5 °C / Inert atmosphere; Darkness

2: iron; acetic acid / tetrahydrofuran; methanol / 3.5 h / 20 °C / Inert atmosphere

3: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

4: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

With N-iodo-succinimide; iron; sodium cyanoborohydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; chloroform; acetonitrile;
DOI:10.1002/chem.201003489