(S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide

Base Information

Chemical Name:(S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide
CAS No.:101460-58-6
Molecular Formula:C₁₅H₂₀BrN₃O₅
Molecular Weight:402.245
Hs Code.:

Synonyms:(S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide

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Technology Process of (S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide

There total 3 articles about (S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84225-86-5
3-bromo-2-hydroxy-6-methoxysalicylic acid

: 101460-58-6
(S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / 65percent aq. HNO₃ / CHCl₃ / 1 h / 30 °C

2: SOCl₂, DMF / toluene / 0.5 h / 70 °C

3: CH₂Cl₂ / 4 h / 23 °C

With thionyl chloride; nitric acid; N,N-dimethyl-formamide; In dichloromethane; chloroform; toluene;
DOI:10.1021/jm00151a010

Reference yield:

: 98527-24-3
3-bromo-5-nitro-6-methoxysalicylic acid

: 101460-58-6
(S)-3-bromo-N-<(1-ethyl-2-pyrrolidinyl)methyl>-6-methoxy-5-nitrosalicylamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, DMF / toluene / 0.5 h / 70 °C

2: CH₂Cl₂ / 4 h / 23 °C

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; toluene;
DOI:10.1021/jm00151a010