5-Chloro-4,3',3'',3'''-tetraoctyl-[2,2';5',2'';5'',2''']quaterthiophene

Base Information

• Chemical Name: 5-Chloro-4,3',3'',3'''-tetraoctyl-[2,2';5',2'';5'',2''']quaterthiophene
• CAS No.: 205105-06-2
• Molecular Formula: C₄₈H₇₃ClS₄
• Molecular Weight: 813.825

Synonyms:5-Chloro-4,3',3'',3'''-tetraoctyl-[2,2';5',2'';5'',2''']quaterthiophene

Chemical Property of 5-Chloro-4,3',3'',3'''-tetraoctyl-[2,2';5',2'';5'',2''']quaterthiophene

Chemical Property:

Purity/Quality:

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Technology Process of 5-Chloro-4,3',3'',3'''-tetraoctyl-[2,2';5',2'';5'',2''']quaterthiophene

There total 1 articles about 5-Chloro-4,3',3'',3'''-tetraoctyl-[2,2';5',2'';5'',2''']quaterthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-octylthiophene (65016-62-8,104934-51-2) → 5-Chloro-4,3',3'',3'''-tetraoctyl-[2,2';5',2'';5'',2''']quaterthiophene (205105-06-2)

Guidance literature:

Multi-step reaction with 7 steps

1: 60 percent / SO₂Cl₂

2: 96 percent / I₂, Hg(OAc)2 / acetic acid

3: 90 percent / 1percent Pd(PPh₃)3, aq. NaHCO₃ / 1,2-dimethoxy-ethane / Heating

4: I₂, Hg(OAc)2 / acetic acid

5: 90 percent / 1percent Pd(PPh₃)3, aq. NaHCO₃ / 1,2-dimethoxy-ethane / Heating

6: I₂, Hg(OAc)2 / acetic acid

7: 90 percent / 1percent Pd(PPh₃)3, aq. NaHCO₃ / 1,2-dimethoxy-ethane / Heating

With sulfuryl dichloride; tris(triphenylphosphano)palladium; mercury(II) diacetate; iodine; sodium hydrogencarbonate; In 1,2-dimethoxyethane; acetic acid;

DOI:10.1051/jcp:1998237

upstream raw materials:

3-octylthiophene

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