Technology Process of C42H50N4O10
There total 6 articles about C42H50N4O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine / chloroform / 15 h / 0 - 20 °C
2: methanol; lithium hydroxide / tetrahydrofuran / 4 h / 65 °C
3: N-ethyl-N,N-diisopropylamine; HATU; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 15 h / 0 - 20 °C
With
methanol; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; lithium hydroxide; 1,1'-azodicarbonyl-dipiperidine;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / 4.17 h / 0 °C / Reflux
2: triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine / chloroform / 15 h / 0 - 20 °C
3: methanol; lithium hydroxide / tetrahydrofuran / 4 h / 65 °C
4: N-ethyl-N,N-diisopropylamine; HATU; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 15 h / 0 - 20 °C
With
methanol; thionyl chloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; lithium hydroxide; 1,1'-azodicarbonyl-dipiperidine;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;