N¹-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Base Information

• Chemical Name: N¹-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine
• CAS No.: 133765-72-7
• Molecular Formula: C₃₁H₄₃N₅O₈
• Molecular Weight: 613.711

Synonyms:N¹-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Chemical Property of N¹-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Chemical Property:

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Technology Process of N¹-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

There total 3 articles about N¹-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N1-<(3-aminobenzen-1-yl)carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine (133765-71-6) + m-nitrobenzoic acid chloride (121-90-4) → N1-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine (133765-72-7)

Guidance literature:

With pyridine; In acetonitrile; for 1h; Ambient temperature;

DOI:10.1016/0223-5234(91)90058-U

Reference yield:

N1,N5-di-boc-spermidine (68076-39-1) → N1-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine (133765-72-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 55 percent / pyridine / acetonitrile / 3 h / Ambient temperature

2: 96 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr / Ambient temperature

3: 92 percent / pyridine / acetonitrile / 1 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In methanol; acetonitrile;

DOI:10.1016/0223-5234(91)90058-U

Reference yield:

N1-<(3-nitrobenzen-1-yl)carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine (133765-70-5) → N1-<<3-(3-nitrobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine (133765-72-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr / Ambient temperature

2: 92 percent / pyridine / acetonitrile / 1 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In methanol; acetonitrile;

DOI:10.1016/0223-5234(91)90058-U

upstream raw materials:

N¹-<(3-aminobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

m-nitrobenzoic acid chloride

N₁,N₅-di-boc-spermidine

N¹-<(3-nitrobenzen-1-yl)carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

Downstream raw materials:

N¹-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine triethylammonium

N¹-<<3-<3-4,N⁸-bis(tert-butoxycarbonyl)spermidinosuccinamido>benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

N¹-<<3-<3-1-(spermidino)succinamido>benzene-1-carboxamido>benzen-1-yl>carbonyl>spermidine tetra(trifluoroacetate)

N¹-<<3-<3-(guanidinoacetamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine hydrochloride

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