(S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide

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Chemical Name:(S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide
CAS No.:1398547-65-3
Molecular Formula:C₂₃H₂₆N₂O₅S
Molecular Weight:442.536
Hs Code.:

Synonyms:(S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide

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Chemical Property of (S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide

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Technology Process of (S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide

There total 3 articles about (S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 2-((1S)-2-bromo-1-(methoxymethoxy)-2-nitroethyl)-1-tosyl-1H-pyrrole

: 1398547-65-3
(S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide

Guidance literature:: With N-iodo-succinimide; potassium carbonate; In 1,2-dimethoxyethane; water; at 0 ℃; for 36h;
DOI:10.1021/ja306225u

Reference yield:

: 1398548-27-0
C₁₃H₁₃BrN₂O₅S

: 1398547-65-3
(S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentoxide / chloroform / 20 °C

2: potassium carbonate; N-iodo-succinimide / 1,2-dimethoxyethane; water / 36 h / 0 °C

With N-iodo-succinimide; phosphorus pentoxide; potassium carbonate; In 1,2-dimethoxyethane; chloroform; water;
DOI:10.1021/ja306225u

Reference yield:

: 102619-05-6
1-(toluene-4-sulfonyl)-1H-pyrrole-2-carbaldehyde

: 1398547-65-3
(S)-2-(methoxymethoxy)-N-((S)-1-phenylethyl)-2-(1-tosyl-1H-pyrrol-2-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,2'-isopropylidenebis[(4S)-4-tert-butyl-2-oxazoline]; Cu(2-IC₆H₄COO)2*H₂O / isopropyl alcohol / 0.17 h / 0 °C

1.2: 192 h / 0 °C

2.1: phosphorus pentoxide / chloroform / 20 °C

3.1: potassium carbonate; N-iodo-succinimide / 1,2-dimethoxyethane; water / 36 h / 0 °C

With N-iodo-succinimide; Cu(2-IC₆H₄COO)2*H₂O; phosphorus pentoxide; potassium carbonate; 2,2'-isopropylidenebis[(4S)-4-tert-butyl-2-oxazoline]; In 1,2-dimethoxyethane; chloroform; water; isopropyl alcohol; 1.1: |Henry Nitro Aldol Condensation / 1.2: |Henry Nitro Aldol Condensation;
DOI:10.1021/ja306225u