1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline

Base Information

Chemical Name:1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline
CAS No.:1034776-99-2
Molecular Formula:C₁₆H₁₅ClN₂O₅S
Molecular Weight:382.825
Hs Code.:

Synonyms:1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline

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Technology Process of 1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline

There total 1 articles about 1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 30450-62-5
7-nitro-1,2,3,4-tetrahydro-quinoline

: 22952-32-5
5-chloro-2-methoxybenzenesulfonyl chloride

: 1034776-99-2
1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 120h;

Reference yield: 35.0%

: 1034776-99-2
1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline

: 1034777-01-9
1-(5-chloro-2-methoxy-benzenesulfonyl)-1,2,3,4-tetrahydro-quinolin-7-ylamine

Guidance literature:: With ammonium chloride; zinc; In 1,2-dimethoxyethane; water; at 15 - 20 ℃; for 1h;

Reference yield:

: 1034776-99-2
1-(5-chloro-2-methoxy-benzenesulfonyl)-7-nitro-1,2,3,4-tetrahydro-quinoline

: 1034776-09-4
{4-[1-(5-chloro-2-methoxy-benzenesulfonyl)-1,2,3,4-tetrahydro-quinolin-7-ylcarbamoyl]-phenyl}-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium chloride; zinc / 1,2-dimethoxyethane; water / 1 h / 15 - 20 °C

2: dmap / tetrahydrofuran / 2.5 h / 75 °C

3: lithium hydroxide; water / tetrahydrofuran; methanol / 4 h / 20 °C

With lithium hydroxide; water; ammonium chloride; zinc; dmap; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water;