N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid

Base Information

Chemical Name:N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid
CAS No.:1571072-87-1
Molecular Formula:C₆H₆O₃S*C₂₄H₂₄FN₃O₂
Molecular Weight:563.65
Hs Code.:

Synonyms:N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid

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Chemical Property of N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid

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Technology Process of N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid

There total 5 articles about N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: KX₂-361

: 98-11-3
benzenesulfonic acid

: 1571072-87-1
N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid

Guidance literature:: In acetonitrile; at 20 - 110 ℃; for 0.433333h; Inert atmosphere;

Reference yield:

: 1571072-91-7
C₁₇H₁₇N₃O

: 1571072-87-1
N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane / 23.01 h / 40 - 50 °C / Large scale

1.2: 0.5 h / 20 °C / pH 8.6 / Large scale

2.1: 60.31 h / 140 °C / Inert atmosphere; Large scale

3.1: acetonitrile / 0.43 h / 20 - 110 °C / Inert atmosphere

With chloro-trimethyl-silane; In acetonitrile;

Reference yield:

: 30483-75-1
4-bromophenyl-morpholine

: 1571072-87-1
N-(3-fluorobenzyl)-2-(5-(4-morpholinophenyl)pyridin-2-yl)acetamide benzenesulfonic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water

2.1: potassium hexamethylsilazane / tetrahydrofuran / 3.06 h / 10 °C / Inert atmosphere; Large scale

3.1: chloro-trimethyl-silane / 23.01 h / 40 - 50 °C / Large scale

3.2: 0.5 h / 20 °C / pH 8.6 / Large scale

4.1: 60.31 h / 140 °C / Inert atmosphere; Large scale

5.1: acetonitrile / 0.43 h / 20 - 110 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; chloro-trimethyl-silane; potassium hexamethylsilazane; sodium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; acetonitrile;