decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline

Base Information

Chemical Name:decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline
CAS No.:93758-07-7
Molecular Formula:C₁₈H₁₉NO₅
Molecular Weight:329.353
Hs Code.:

Synonyms:decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline

Chemical Property:

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Technology Process of decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline

There total 4 articles about decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 93758-06-6
1,2,3,4,6,7,8,9-octahydro-1,6-dioxo-2-benzyl-9-carbethoxyisoquinoline

: 93758-07-7
decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol; at 10 - 20 ℃; for 2.5h;
DOI:10.1021/jo00202a014

Reference yield:

: 93758-46-4
methyl 1-benzyl-2,4-dioxo-3-piperidinecarboxylate

: 93758-07-7
decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

2: acetic acid, water, sodium acetate / benzene / 3 h / Heating

3: 84 percent / 30percent H₂O₂, aq. NaOH / methanol / 2.5 h / 10 - 20 °C

With sodium hydroxide; water; dihydrogen peroxide; sodium acetate; acetic acid; In methanol; benzene;
DOI:10.1021/jo00202a014

Reference yield:

: 216372-98-4
methyl N-(benzyl)-N-(methylmalonoyl)-3-aminopropionate

: 93758-07-7
decahydro-1,6-dioxo-2-benzyl-5,10-epoxy-9-carbethoxyisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / benzene; ethanol

3: acetic acid, water, sodium acetate / benzene / 3 h / Heating

4: 84 percent / 30percent H₂O₂, aq. NaOH / methanol / 2.5 h / 10 - 20 °C

With sodium hydroxide; water; dihydrogen peroxide; sodium acetate; sodium hydride; acetic acid; In methanol; ethanol; benzene;
DOI:10.1021/jo00202a014