1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide

Base Information

Chemical Name:1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide
CAS No.:1287690-40-7
Molecular Formula:C₃₄H₃₅N₃O₂S
Molecular Weight:549.737
Hs Code.:

Synonyms:1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide

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Chemical Property of 1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide

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Technology Process of 1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide

There total 3 articles about 1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1287741-87-0,1287690-30-5
1,13-dimethoxy-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine

: 103-72-0
phenyl isothiocyanate

: 1287690-40-7
1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide

Guidance literature:: 1,13-dimethoxy-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine; With n-butyllithium; In diethyl ether; at -78 - 0 ℃; Inert atmosphere;

phenyl isothiocyanate; In diethyl ether; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/jo200071n

Reference yield:

: tris(2,6-dimethoxyphenyl)carbenium tetrafluoroborate

: 1287690-40-7
1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-methyl-pyrrolidin-2-one / 3 h / 25 - 90 °C

2.1: sodium tetrahydroborate / ethanol / 25 °C / Inert atmosphere

3.1: n-butyllithium / diethyl ether / -78 - 0 °C / Inert atmosphere

3.2: 0.33 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; In 1-methyl-pyrrolidin-2-one; diethyl ether; ethanol;
DOI:10.1021/jo200071n

Reference yield:

: 1,13-dimethoxy-5,9-dipropyl-5,9-dihydro-13bH-quinolino[2,3,4-kl]acridin-13b-ylium tetrafluoroborate

: 1287690-40-7
1,13-dimethoxy-N-phenyl-5,9-dipropyl-9,13b-dihydro-5H-quinolino[2,3,4-kl]acridine-13b-carbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / ethanol / 25 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether / -78 - 0 °C / Inert atmosphere

2.2: 0.33 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; In diethyl ether; ethanol;
DOI:10.1021/jo200071n