allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside
CAS No.:914097-65-7
Molecular Formula:C₅₀H₄₆O₁₅
Molecular Weight:886.906
Hs Code.:

Synonyms:allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

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Chemical Property of allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

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Technology Process of allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

There total 6 articles about allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₁H₄₅F₃O₁₇S

: 914097-65-7
allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

Guidance literature:: With potassium nitrite; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1021/ol062199b

Reference yield:

: 914097-59-9
allyl 4,6-O-benzylidene-3-O-(4-methoxybenzyl)-β-D-galactopyranosyl-(1,4)-β-D-glucopyranoside

: 914097-65-7
allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / pyridine; DMAP / 20 °C

2: 72 percent Turnov_. / DDQ / CH₂Cl₂; H₂O / 2 h

3: pyridine / CH₂Cl₂ / 0.17 h / -40 °C

4: KNO₂ / dimethylformamide / 50 °C

With pyridine; dmap; potassium nitrite; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol062199b

Reference yield:

: 914097-63-5
allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

: 914097-65-7
allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-gulopyranosyl-(1,4)-2,3,6-O-tri-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 0.17 h / -40 °C

2: KNO₂ / dimethylformamide / 50 °C

With pyridine; potassium nitrite; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol062199b