methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

Base Information

Chemical Name:methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate
CAS No.:149046-22-0
Molecular Formula:C₂₂H₁₈N₂O₅S
Molecular Weight:422.461
Hs Code.:

Synonyms:methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

Suppliers and Price of methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

There total 7 articles about methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 137-07-5
2-amino-benzenethiol

: 149046-18-4
methyl 1-(4-acetoxyphenyl)-6-(formyl)-1,4-dihydro-4-oxonicotinate

: 149046-22-0
methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

Guidance literature:: In toluene; for 4h; Heating;

Reference yield:

: 123-30-8
4-amino-phenol

: 149046-22-0
methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) EtONa / 1.) EtOH, RT, 2 h, 2.) EtOH, reflux, overnight

2: 85.1 percent / SOCl₂ / 10 h / Heating

3: 34.2 percent / 4 h / 100 °C

4: 1.) SeO₂, 2.) charcoal / 1.) dioxane, 80 deg C, overnight, 2.) reflux, 1 h

5: 97 percent / SiO₂ / acetone / 2 h

6: 57 percent / toluene / 4 h / Heating

With selenium(IV) oxide; thionyl chloride; sodium ethanolate; silica gel; pyrographite; In acetone; toluene;

Reference yield:

: 181277-21-4
3-(dimethylaminomethine)-4-oxo-6-methyl-2-pyrone

: 149046-22-0
methyl 1-(4-acetoxyphenyl)-6-(2-benzothiazolydinyl)-1,4-dihydro-4-oxonicotinate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) EtONa / 1.) EtOH, RT, 2 h, 2.) EtOH, reflux, overnight

2: 85.1 percent / SOCl₂ / 10 h / Heating

3: 34.2 percent / 4 h / 100 °C

4: 1.) SeO₂, 2.) charcoal / 1.) dioxane, 80 deg C, overnight, 2.) reflux, 1 h

5: 97 percent / SiO₂ / acetone / 2 h

6: 57 percent / toluene / 4 h / Heating

With selenium(IV) oxide; thionyl chloride; sodium ethanolate; silica gel; pyrographite; In acetone; toluene;