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(π-1-methylallyl)(dimethylphenylphosphine)palladium formate

Base Information
  • Chemical Name:(π-1-methylallyl)(dimethylphenylphosphine)palladium formate
  • CAS No.:132884-84-5
  • Molecular Formula:C13H19O2PPd
  • Molecular Weight:344.686
  • Hs Code.:
(π-1-methylallyl)(dimethylphenylphosphine)palladium formate

Synonyms:(π-1-methylallyl)(dimethylphenylphosphine)palladium formate

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Chemical Property of (π-1-methylallyl)(dimethylphenylphosphine)palladium formate
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Technology Process of (π-1-methylallyl)(dimethylphenylphosphine)palladium formate

There total 2 articles about (π-1-methylallyl)(dimethylphenylphosphine)palladium formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In dichloromethane; under inert atmosphere; 1) addn. of phosphine at -10°C, then stirring for 30 min at room temp.; 2) addn. of HCO2Ag to soln. of Pd complex at -40°C, stirring at -20°C for 2 h in the dark; filtration (celite, -50°C), evapn.;
DOI:10.1246/bcsj.73.453
Guidance literature:
In (2)H8-toluene; Pd-complex treated with a soln. of P- and Ag-compound at -30°C;
Guidance literature:
byproducts: CO2; decopose rapidly at room temp.; (1)H-NMR; GC; Kinetics;
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