3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

Base Information

Chemical Name:3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>
CAS No.:170474-92-7
Molecular Formula:C₇₄H₈₂O₁₀Si
Molecular Weight:1159.54
Hs Code.:

3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

Synonyms:3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

Suppliers and Price of 3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

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Chemical Property of 3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

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Technology Process of 3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

There total 1 articles about 3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-<(trimethylsilyl)ethynyl>-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-...)>>

: 170474-92-7
3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

Guidance literature:: With potassium carbonate; In methanol; for 6.5h; Ambient temperature;
DOI:10.1002/hlca.19950780319

Reference yield: 99.0%

: 170474-92-7
3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

: 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-<2-(trimethylsilyl)ethynyl>-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-D-glycero-D-gulo-octitol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; -90 to 3 degC, 5 h, 3 to 10 degC, 3 h;
DOI:10.1002/hlca.19950780319

Reference yield: 99.0%

: 170474-92-7
3,7-anhydro-6-C-(5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-ethynyl-D-glycero-D-gulo-decitol-1-yl)-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<<1,1-dimethyl-3-(tetrahydro-2H-pyran-2-yloxy)...>>

: 3,7-anhydro-6-C-<5,9-anhydro-6,7,10-tri-O-benzyl-1,1,2,2,3,3,4,4-octadehydro-1,2,3,4,8-pentadeoxy-8-C-<(trimethylsilyl)ethynyl>-D-glycero-D-gulo-decitol-1-yl>-4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-1-C-<(3-hydroxy-1,1-dimethylpropyl)...>

Guidance literature:: With Amberlyst 15 (H(+)-form); In methanol; dichloromethane; for 96.5h; Ambient temperature;
DOI:10.1002/hlca.19950780319