(Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene

Base Information

Chemical Name:(Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene
CAS No.:102922-56-5
Molecular Formula:C₂₄H₄₆O₅Si₂
Molecular Weight:470.797
Hs Code.:

(Z)-2-acethoxy-1-(<(1β,2α)-2-(<dimethyl(1,1-dimethylethyl)silyl>oxy)-1-cyclohexyl>oxy)-3-(<dimethyl(1,1-dimethylethyl)silyl>oxy)-1,3-butadiene

Synonyms:(Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene

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Chemical Property of (Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene

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Technology Process of (Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene

There total 4 articles about (Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 102922-55-4
(Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-1-buten-3-one

: 102922-56-5
(Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene

Guidance literature:: With triethylamine; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1021/ja00274a049

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 102922-56-5
(Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / triethylamine / CH₂Cl₂ / 2 h / -78 °C

2: 70 percent / pyridinium p-toluenesulfonate / benzene / 30 h / Heating

3: 80 percent / triethylamine / diethyl ether / 1 h / 0 °C

With pyridinium p-toluenesulfonate; triethylamine; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/ja00274a049

Reference yield:

: 1460-57-7
trans-1,2-cyclohexandiol

: 102922-56-5
(Z)-2-acethoxy-1-(<(1β,2α)-2-(oxy)-1-cyclohexyl>oxy)-3-(oxy)-1,3-butadiene

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / triethylamine / CH₂Cl₂ / 2 h / -78 °C

2: 70 percent / pyridinium p-toluenesulfonate / benzene / 30 h / Heating

3: 80 percent / triethylamine / diethyl ether / 1 h / 0 °C

With pyridinium p-toluenesulfonate; triethylamine; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/ja00274a049