methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

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Chemical Name:methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate
CAS No.:1075191-18-2
Molecular Formula:C₂₃H₃₃N₃O₃
Molecular Weight:399.533
Hs Code.:

Synonyms:methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

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Chemical Property of methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

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Technology Process of methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

There total 1 articles about methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 37792-68-0
methyl (S)-2-amino-3-(1-methyl-1H-imidazol-5-yl)propanoate dihydrochloride

: 16225-26-6
3,5-di-tert-butylbenzoic acid

: 1075191-18-2
methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

Guidance literature:: 3,5-di-tert-butylbenzoic acid; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h; Inert atmosphere;

methyl (S)-2-amino-3-(1-methyl-1H-imidazol-5-yl)propanoate dihydrochloride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/jo801859m

Reference yield: 81.0%

: 1075191-18-2
methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

: 1075191-26-2
methyl (S)-2-(3,5-di-tert-butylphenylthioamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

Guidance literature:: With Lawessons reagent; In dichloromethane; toluene; at 80 ℃; for 4h;
DOI:10.1021/jo801859m

Reference yield:

: 1075191-18-2
methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate

: C₂₂H₃₁N₃O₃

Guidance literature:: methyl (S)-2-(3,5-di-tert-butylbenzamido)-3-(1-methyl-1H-imidazol-5-yl)propanoate; With lithium hydroxide; water; In methanol; at 20 ℃; for 2h;

With hydrogenchloride; In water; pH=4 - 5;
DOI:10.1021/jo801859m