C₄₀H₇₄INO₈Si₂

Base Information

Chemical Name:C₄₀H₇₄INO₈Si₂
CAS No.:1591927-98-8
Molecular Formula:C₄₀H₇₄INO₈Si₂
Molecular Weight:880.105
Hs Code.:

C<sub>40</sub>H<sub>74</sub>INO<sub>8</sub>Si<sub>2</sub>

Synonyms:C₄₀H₇₄INO₈Si₂

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Chemical Property of C₄₀H₇₄INO₈Si₂

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Technology Process of C₄₀H₇₄INO₈Si₂

There total 20 articles about C₄₀H₇₄INO₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: C₇H₁₄INO₂

: 1591927-28-4
C₃₉H₇₁NO₆S₂Si₂

: 1591927-98-8
C₄₀H₇₄INO₈Si₂

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 20 - 45 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol5008179

Reference yield:

: C₂₀H₃₇NO₄Si

: 1591927-98-8
C₄₀H₇₄INO₈Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran; toluene / 0 - 20 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

3.2: 3 h / 0 - 20 °C / Inert atmosphere

4.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere

4.2: 0.25 h / 0 °C / Inert atmosphere

5.1: 1H-imidazole / tetrahydrofuran / 24 h / 20 - 45 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; zirconocene dichloride; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; 1,4-dioxane; toluene; mineral oil;
DOI:10.1021/ol5008179

Reference yield:

: 1591927-39-7
C₂₀H₃₈INO₄Si

: 1591927-98-8
C₄₀H₇₄INO₈Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

2.2: 3 h / 0 - 20 °C / Inert atmosphere

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere

3.2: 0.25 h / 0 °C / Inert atmosphere

4.1: 1H-imidazole / tetrahydrofuran / 24 h / 20 - 45 °C / Inert atmosphere

With 1H-imidazole; hydrogenchloride; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; 1,4-dioxane; mineral oil;
DOI:10.1021/ol5008179