(4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide

Base Information

• Chemical Name: (4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide
• CAS No.: 790297-80-2
• Molecular Formula: C₂₄H₂₆F₂N₂O₅
• Molecular Weight: 460.478

Synonyms:(4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide

Chemical Property of (4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide

Chemical Property:

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Technology Process of (4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide

There total 2 articles about (4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1-(2-azido-ethyl)-4-{4-methoxy-3-[(R)-(tetrahydro-furan-3-yl)oxy]-phenyl}-pyrrolidin-2-one + 2,3-difluorobenzoic acid (4519-39-5) → (4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide (790297-80-2)

Guidance literature:

2,3-difluorobenzoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 ℃; for 0.5h;

(S)-1-(2-azido-ethyl)-4-{4-methoxy-3-[(R)-(tetrahydro-furan-3-yl)oxy]-phenyl}-pyrrolidin-2-one; With tributylphosphine; In tetrahydrofuran; at 20 ℃;

Reference yield:

(S)-1-(2-azido-ethyl)-4-{4-methoxy-3-[(R)-(tetrahydro-furan-3-yl)oxy]-phenyl}-pyrrolidin-2-one → (4S)-2,3-difluoro-4-[4-methoxy-3-(3R)-tetrahydrofuranyloxyphenyl]-N-[2-(2-oxopyrrolidin-1-yl)ethyl]-benzamide (790297-80-2)

Guidance literature:

2,3-difluorobenzoic acid; With benzotriazol-1-ol; diisopropyl-carbodiimide; In tetrahydrofuran; at 0 ℃; for 0.5h;

(S)-1-(2-azido-ethyl)-4-{4-methoxy-3-[(R)-(tetrahydro-furan-3-yl)oxy]-phenyl}-pyrrolidin-2-one; In tetrahydrofuran; at 20 ℃;

upstream raw materials:

2,3-difluorobenzoic acid

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