N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide

Base Information

• Chemical Name: N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide
• CAS No.: 198836-49-6
• Molecular Formula: C₁₄H₂₀N₂O₅S
• Molecular Weight: 328.389

Synonyms:N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide

Chemical Property of N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide

Chemical Property:

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Technology Process of N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide

There total 3 articles about N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

allyl bromide (106-95-6) + (S)-N-(1-hydroxy-3-methylbutan-2-yl)-2-nitrobenzenesulfonamide (198836-48-5) → N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide (198836-49-6)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(97)10015-1

Reference yield:

(S)-valinol (2026-48-4,473-75-6) → N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide (198836-49-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / triethylamine / CH₂Cl₂ / Ambient temperature

2: 83 percent / cesium carbonate / dimethylformamide

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(97)10015-1

Reference yield:

2-Nitrobenzenesulfonyl chloride (1694-92-4) → N-Allyl-N-((S)-1-hydroxymethyl-2-methyl-propyl)-2-nitro-benzenesulfonamide (198836-49-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / triethylamine / CH₂Cl₂ / Ambient temperature

2: 83 percent / cesium carbonate / dimethylformamide

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(97)10015-1

upstream raw materials:

allyl bromide

(S)-N-(1-hydroxy-3-methylbutan-2-yl)-2-nitrobenzenesulfonamide

(S)-valinol

2-Nitrobenzenesulfonyl chloride

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