C₃₇H₂₇N

Base Information

• Chemical Name: C₃₇H₂₇N
• CAS No.: 1242178-13-7
• Molecular Formula: C₃₇H₂₇N
• Molecular Weight: 485.628
• Mol file: 1242178-13-7.mol

Synonyms:C₃₇H₂₇N

Chemical Property of C₃₇H₂₇N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₇H₂₇N

There total 1 articles about C₃₇H₂₇N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethyl 4,13-dihydro-5,12-diphenyl-4,13-ethano-2H-fluorantho[8,9-f]isoindole-1-carboxylate (1226965-82-7) → C37H27N (1242178-13-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; Inert atmosphere; Reflux;

DOI:10.1016/j.tet.2010.06.045

Reference yield:

1-acetyl-4,7-ethano-3-methyl-4,7-dihydro-2H-isoindole (1242178-19-3) + C37H27N (1242178-13-7) → C50H41BF2N2

Guidance literature:

1-acetyl-4,7-ethano-3-methyl-4,7-dihydro-2H-isoindole; C₃₇H₂₇N; With trichlorophosphate; In chloroform; at 20 ℃; Reflux; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In chloroform; for 2h; Reflux;

With boron trifluoride diethyl etherate; In chloroform; for 6h; Reflux;

DOI:10.1016/j.tet.2010.06.045

Reference yield:

N,N-dimethyl acetamide (127-19-5,116057-81-9) + C37H27N (1242178-13-7) → C39H29NO (1242178-14-8)

Guidance literature:

N,N-dimethyl acetamide; With trichlorophosphate; at 0 ℃; for 0.5h; Inert atmosphere;

C₃₇H₂₇N; In dichloromethane; at 0 ℃; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2010.06.045

upstream raw materials:

ethyl 4,13-dihydro-5,12-diphenyl-4,13-ethano-2H-fluorantho[8,9-f]isoindole-1-carboxylate

Downstream raw materials:

C₃₉H₂₉NO