(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid

Base Information

Chemical Name:(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid
CAS No.:1357108-45-2
Molecular Formula:C₃₇H₃₂N₂O₄
Molecular Weight:568.672
Hs Code.:

Synonyms:(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid

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Chemical Property of (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid

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Technology Process of (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid

There total 3 articles about (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 76-83-5
trityl chloride

: 181954-34-7
3-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: 1357108-45-2
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid

Guidance literature:: 3-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; With chloro-trimethyl-silane; In dichloromethane; for 4h; Reflux;

trityl chloride; With pyridine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1002/cbic.201800170

Reference yield:

: C₂₁H₂₆N₂O₄Si

: 76-83-5
trityl chloride

: 1357108-45-2
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm201195m

Reference yield:

: 181954-34-7
3-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: 1357108-45-2
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(tritylamino)propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; dichloromethane / 2 h / Reflux

2: triethylamine / tetrahydrofuran; dichloromethane / 1 h / 20 °C

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm201195m