N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

Base Information

Chemical Name:N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester
CAS No.:84980-07-4
Molecular Formula:C₃₀H₃₇N₇O₈
Molecular Weight:623.666
Hs Code.:

N-<6-<<N-benzyloxycarbonyl-N-<(S)-2-<(t-butoxycarbonyl)-amino>-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

Synonyms:N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

Chemical Property:

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Technology Process of N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

There total 5 articles about N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69950-65-8
methyl 6-formylpicolinate

: 84980-07-4
N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: acetonitrile / 12 h / 25 °C / activated molecular sieve

2: hydrogen / 5percent Pd-C / methanol

3: 88 percent / 0.1 N NaOH / CH₂Cl₂ / 3 h / 25 °C

4: 0.1 N LiOH / 1.) 0 deg C, 30 min, 2.) 25 deg C, 1 h

5: 1.) N,N'-carbonyldiimidazole / 1.) THF, 0 deg C, 1 h, 2.) 25 deg C, 12 h

With lithium hydroxide; sodium hydroxide; hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja00413a047

Reference yield:

: 75452-33-4
Boc-Dap(NH₂)-CONH₂

: 84980-07-4
N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: acetonitrile / 12 h / 25 °C / activated molecular sieve

2: hydrogen / 5percent Pd-C / methanol

3: 88 percent / 0.1 N NaOH / CH₂Cl₂ / 3 h / 25 °C

4: 0.1 N LiOH / 1.) 0 deg C, 30 min, 2.) 25 deg C, 1 h

5: 1.) N,N'-carbonyldiimidazole / 1.) THF, 0 deg C, 1 h, 2.) 25 deg C, 12 h

With lithium hydroxide; sodium hydroxide; hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja00413a047

Reference yield:

: 80109-35-9,143634-47-3
6-{[(E)-(S)-2-tert-Butoxycarbonylamino-2-carbamoyl-ethylimino]-methyl}-pyridine-2-carboxylic acid methyl ester

: 84980-07-4
N-<6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carbonyl>-L-histidine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / 5percent Pd-C / methanol

2: 88 percent / 0.1 N NaOH / CH₂Cl₂ / 3 h / 25 °C

3: 0.1 N LiOH / 1.) 0 deg C, 30 min, 2.) 25 deg C, 1 h

4: 1.) N,N'-carbonyldiimidazole / 1.) THF, 0 deg C, 1 h, 2.) 25 deg C, 12 h

With lithium hydroxide; sodium hydroxide; hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00413a047